529-0144-01L  NMR Spectroscopy in Inorganic Chemistry

SemesterSpring Semester 2022
LecturersR. Verel
Periodicityyearly recurring course
Language of instructionEnglish



Courses

NumberTitleHoursLecturers
529-0144-01 GNMR Spectroscopy in Inorganic Chemistry3 hrs
Wed12:45-15:30HCI J 6 »
R. Verel

Catalogue data

AbstractTheory and applications of NMR spectroscopy with a focus of its use to problems in Inorganic Chemistry.
The use of the Bloch Equations to describe broadband and selective excitation, measurement techniques and processing strategies of NMR data, applications of NMR to the study of molecular structure, chemical exchange processes, diffusion spectroscopy, and solid-state NMR techniques.
Learning objectiveIn depth understanding of both practical and theoretical aspects of solution and solid-state NMR and its application to problems in Inorganic Chemistry
ContentSelection of the following themes:
1. Bloch Equations and its use to understand broadband and selective pulses.
2. Measurement techniques and processing strategies of NMR data.
3. Applications of NMR to the study of molecular structure: Experiments and strategies to solve problems in Inorganic Chemistry.
4. Application of NMR to the study of chemical exchange processes.
5. Application of NMR to the study of self-diffusion and the determination of diffusion coefficients.
6. Differences and similarities between fundamental interactions in solution and solid-state NMR
7. Experimental techniques in solid-state NMR (Magic Angle Spinning, Cross Polarization, Decoupling and Recoupling Techniques, MQMAS)
8. The use of Dynamic Nuclear Polarization for the study of surfaces.
Lecture notesA handout is provided during the lectures. It is expected that the students will consult the accompanying literature as specified during the lecture.
LiteratureSpecified during the lecture
Prerequisites / Notice529-0432-00 Physikalische Chemie IV: Magnetische Resonanz
529-0058-00 Analytische Chemie II
(or equivalent)

The individual and in depth (literature) study of a theme related but separate from the themes presented during the lecture requires different compentences compared to the ones which are tested during the oral exam. Therefore the students must give a presentation during the semester about a theme based on their study of the literature. A list of possible themes and corresponding literature will be provided during the lecture.
The student presentation is a mandatory "pass/fail" element of the course and must be passed separately from the oral exam. If the presentation fails it will not be possible to pass the final exam. A renewed presentation is not required in case the oral exam has to be repeated.
CompetenciesCompetencies
Subject-specific CompetenciesConcepts and Theoriesassessed
Techniques and Technologiesassessed
Method-specific CompetenciesAnalytical Competenciesassessed

Performance assessment

Performance assessment information (valid until the course unit is held again)
Performance assessment as a semester course
ECTS credits6 credits
ExaminersR. Verel
Typesession examination
Language of examinationEnglish
RepetitionThe performance assessment is offered every session. Repetition possible without re-enrolling for the course unit.
Mode of examinationoral 30 minutes
Additional information on mode of examinationThe student must give a presentation during the semester about a theme based on their study of the literature. A list of possible themes and corresponding literature will be provided during the lecture.
The student presentation is a mandatory „pass/fail“ element of the course and must be passed separately from the oral exam. If the presentation fails it will not be possible to pass the final exam. A renewed presentation is not required in case the oral exam has to be repeated.
This information can be updated until the beginning of the semester; information on the examination timetable is binding.

Learning materials

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Only public learning materials are listed.

Groups

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Restrictions

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Offered in

ProgrammeSectionType
Chemistry MasterInorganic ChemistryWInformation
Doctorate Chemistry and Applied BiosciencesInorganic ChemistryWInformation