529-0051-00L Analytical Chemistry I
| Semester | Autumn Semester 2020 |
| Lecturers | D. Günther, M.‑O. Ebert, G. Schwarz, R. Zenobi |
| Periodicity | yearly recurring course |
| Language of instruction | German |
Courses
| Number | Title | Hours | Lecturers | |||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| 529-0051-00 G | Analytische Chemie I Zusätzliche Präsenzveranstaltungen am 17.09.20 und 17.12.20, jeweils 07:45 - 08:30 Uhr. Die genauen Unterrichtszeiten von ONLINE - Veranstaltungen werden von den Dozierenden kommuniziert. | 3 hrs |
| D. Günther, M.‑O. Ebert, G. Schwarz, R. Zenobi |
Catalogue data
| Abstract | Introduction into the most important spectroscopical methods and their applications to gain structural information. |
| Learning objective | Knowledge about the necessary theoretical background of spectroscopical methods and their practical applications |
| Content | Application oriented basics of organic and inorganic instrumental analysis and of the empirical employment of structure elucidation methods: Mass spectrometry: Ionization methods, mass separation, isotope signals, rules of fragmentation, rearrangements. NMR spectroscopy: Experimental basics, chemical shift, spin-spin coupling. IR spectroscopy: Revisiting topics like harmonic oscillator, normal vibrations, coupled oscillating systems (in accordance to the basics of the related lecture in physical chemistry); sample preparation, acquisition techniques, law of Lambert and Beer, interpretation of IR spectra; Raman spectroscopy. UV/VIS spectroscopy: Basics, interpretation of electron spectra. Circular dichroism (CD) und optical rotation dispersion (ORD). Atomic absorption, emission, and X-ray fluorescence spectroscopy: Basics, sample preparation. |
| Lecture notes | Script will be for the production price |
| Literature | - R. Kellner, J.-M. Mermet, M. Otto, H. M. Widmer (Eds.) Analytical Chemistry, Wiley-VCH, Weinheim, 1998; - D. A. Skoog und J. J. Leary, Instrumentelle Analytik, Springer, Heidelberg, 1996; - M. Hesse, H. Meier, B. Zeeh, Spektroskopische Methoden in der organischen Chemie, 5. überarbeitete Auflage, Thieme, Stuttgart, 1995 - E. Pretsch, P. Bühlmann, C. Affolter, M. Badertscher, Spektroskopische Daten zur Strukturaufklärung organischer verbindungen, 4. Auflage, Springer, Berlin/Heidelberg, 2001- Kläntschi N., Lienemann P., Richner P., Vonmont H: Elementanalytik. Instrumenteller Nachweis und Bestimmung von Elementen und deren Verbindungen. Spektrum Analytik, 1996, Hardcover, 339 S., ISBN 3-86025-134-1. |
| Prerequisites / Notice | Excercises are integrated in the lectures. In addition, attendance in the lecture 529-0289-00 "Instrumental analysis of organic compounts" (4th semester) is recommended. |
Performance assessment
| Performance assessment information (valid until the course unit is held again) | |
Performance assessment as a two-semester course together with 529-0058-00L Analytical Chemistry II
(next semester)
| |
| For programme regulations (Examination block) | Bachelor's Degree Programme in Biochemistry - Chemical Biology 2020; Version 28.11.2022 (Examination Block I) Bachelor's Degree Programme in Chemical Engineering 2006; Version 27.03.2018 (Examination Block I) Bachelor's Degree Programme in Chemical Engineering 2018; Version 26.09.2022 (Examination Block I) Bachelor's Degree Programme in Chemistry 2005; Version 27.03.2018 (Examination Block I) Bachelor's Degree Programme in Chemistry 2018; Version 26.09.2022 (Examination Block I) |
| ECTS credits | 6 credits |
|
Performance assessment as a semester course
(other programmes)
| |
| In examination block for | Bachelor's Degree Programme in Materials Science 2017; Version 28.01.2020 (Examination Block 1) Bachelor's Programme in Materials Science 2015; Version 22.08.2017 (Examination Block 1) |
| ECTS credits | 3 credits |
| Examiners | D. Günther, M.-O. Ebert, G. Schwarz, R. Zenobi |
| Type | session examination |
| Language of examination | German |
| Repetition | The performance assessment is offered every session. Repetition possible without re-enrolling for the course unit. |
| Mode of examination | written 60 minutes |
| Written aids | Alle, ausser Computer und Telekommunikation. Taschenrechner erlaubt. |
| If the course unit is part of an examination block, the credits are allocated for the successful completion of the whole block. This information can be updated until the beginning of the semester; information on the examination timetable is binding. | |
Learning materials
| No public learning materials available. | |
| Only public learning materials are listed. |
Groups
| No information on groups available. |
Restrictions
| There are no additional restrictions for the registration. |
