Detlef Günther: Catalogue data in Autumn Semester 2020

Name Prof. Dr. Detlef Günther
Name variantsDetlef Günther
Detlef Guenther
Detlef Gunther
FieldSpurenelement- und Mikroanalytik
Address
Spurenelement- und Mikroanalytik
ETH Zürich, HCI G 113
Vladimir-Prelog-Weg 1-5/10
8093 Zürich
SWITZERLAND
Telephone+41 44 632 46 87
E-mailguenther@inorg.chem.ethz.ch
DepartmentChemistry and Applied Biosciences
RelationshipFull Professor

NumberTitleECTSHoursLecturers
529-0041-00LModern Mass Spectrometry, Hyphenated Methods, and Chemometrics6 credits3GR. Zenobi, M. Badertscher, D. Günther, B. Hattendorf, P. Sinués Martinez-Lozano
AbstractModern mass spectrometry, hyphenated analytical methods, speciation, methods of surface analysis, chemometrics.
Learning objectiveComprehensive knowledge about the analytical methods introduced in this course, and their applications.
ContentCoupling of separation with identification methods such as GC-MS, LC-MS, GC-IR, LC-IR, LC-NMR etc.; importance of speciation.
Modern mass spectrometry: Time of flight and ion cyclotron resonance mass spectrometry, ICP-MS. Soft ionization methods, desorption methods, spray methods.
Methods of surface analysis (ESCA, Auger, SIMS, raster microscopy methods).
Employment of computer science for processing data in chemical analysis (chemometrics).
Lecture noteslecture notes will be available in the lecture at production cost.
Literatureinformation about relevant literature will be available in the lecture & in the lecture notes.
Prerequisites / NoticeExercises are an integral part of the lecture.
Prerequisites:
529-0051-00 "Analytische Chemie I (3. Semester)"
529-0058-00 "Analytische Chemie II (4. Semester)"
(or equivalent)
529-0043-01LAnalytical Strategy Information 6 credits3GR. Zenobi, M. Badertscher, K. Eyer, S. Giannoukos, D. Günther
AbstractProblem-oriented development of analytical strategies and solutions.
Learning objectiveAbility to create solutions for particular analytical problems.
ContentIndividual development of strategies for the optimal application of chemical, biochemical, and physico-chemical methods in analytical chemistry solving predefined problems. Experts from industry and administration present particular problems in their field of activity.
Principles of sampling.
Design and application of microanalytical systems.
Lecture notesCopies of problem sets and solutions will be distributed free fo charge
Prerequisites / NoticePrerequisites:
529-0051-00 "Analytical Chemistry I (3. Semester)"
529-0058-00 "Analytical Chemistry II (4. Semester)"
(or equivalent)
529-0051-AALAnalytical Chemistry I
Enrolment ONLY for MSc students with a decree declaring this course unit as an additional admission requirement.

Any other students (e.g. incoming exchange students, doctoral students) CANNOT enrol for this course unit.
3 credits6RD. Günther, R. Zenobi
AbstractIntroduction into the most important spectroscopical methods and their applications to gain structural information.
Learning objectiveKnowledge about the necessary theoretical background of spectroscopical methods and their practical applications
ContentApplication oriented basics of organic and inorganic instrumental analysis and of the empirical employment of structure elucidation methods:
Mass spectrometry: Ionization methods, mass separation, isotope signals, rules of fragmentation, rearrangements.
NMR spectroscopy: Experimental basics, chemical shift, spin-spin coupling.
IR spectroscopy: Revisiting topics like harmonic oscillator, normal vibrations, coupled oscillating systems (in accordance to the basics of the related lecture in physical chemistry); sample preparation, acquisition techniques, law of Lambert and Beer, interpretation of IR spectra; Raman spectroscopy.
UV/VIS spectroscopy: Basics, interpretation of electron spectra. Circular dichroism (CD) und optical rotation dispersion (ORD).
Atomic absorption, emission, and X-ray fluorescence spectroscopy: Basics, sample preparation.
Lecture notesScript will be provided for the production price
Literature- R. Kellner, J.-M. Mermet, M. Otto, H. M. Widmer (Eds.) Analytical Chemistry, Wiley-VCH, Weinheim, 1998;
- D. A. Skoog und J. J. Leary, Instrumentelle Analytik, Springer, Heidelberg, 1996;
- M. Hesse, H. Meier, B. Zeeh, Spektroskopische Methoden in der organischen Chemie, 5. überarbeitete Auflage, Thieme, Stuttgart, 1995
- E. Pretsch, P. Bühlmann, C. Affolter, M. Badertscher, Spektroskopische Daten zur Strukturaufklärung organischer verbindungen, 4. Auflage, Springer, Berlin/Heidelberg, 2001-
Kläntschi N., Lienemann P., Richner P., Vonmont H: Elementanalytik. Instrumenteller Nachweis und Bestimmung von Elementen und deren Verbindungen. Spektrum Analytik, 1996, Hardcover, 339 S., ISBN 3-86025-134-1.
Prerequisites / NoticeExcercises are integrated in the lectures. In addition, attendance in the lecture 529-0289-00 "Instrumental analysis of organic compounts" (4th semester) is recommended.
529-0051-00LAnalytical Chemistry I3 credits3GD. Günther, M.‑O. Ebert, G. Schwarz, R. Zenobi
AbstractIntroduction into the most important spectroscopical methods and their applications to gain structural information.
Learning objectiveKnowledge about the necessary theoretical background of spectroscopical methods and their practical applications
ContentApplication oriented basics of organic and inorganic instrumental analysis and of the empirical employment of structure elucidation methods:
Mass spectrometry: Ionization methods, mass separation, isotope signals, rules of fragmentation, rearrangements.
NMR spectroscopy: Experimental basics, chemical shift, spin-spin coupling.
IR spectroscopy: Revisiting topics like harmonic oscillator, normal vibrations, coupled oscillating systems (in accordance to the basics of the related lecture in physical chemistry); sample preparation, acquisition techniques, law of Lambert and Beer, interpretation of IR spectra; Raman spectroscopy.
UV/VIS spectroscopy: Basics, interpretation of electron spectra. Circular dichroism (CD) und optical rotation dispersion (ORD).
Atomic absorption, emission, and X-ray fluorescence spectroscopy: Basics, sample preparation.
Lecture notesScript will be for the production price
Literature- R. Kellner, J.-M. Mermet, M. Otto, H. M. Widmer (Eds.) Analytical Chemistry, Wiley-VCH, Weinheim, 1998;
- D. A. Skoog und J. J. Leary, Instrumentelle Analytik, Springer, Heidelberg, 1996;
- M. Hesse, H. Meier, B. Zeeh, Spektroskopische Methoden in der organischen Chemie, 5. überarbeitete Auflage, Thieme, Stuttgart, 1995
- E. Pretsch, P. Bühlmann, C. Affolter, M. Badertscher, Spektroskopische Daten zur Strukturaufklärung organischer verbindungen, 4. Auflage, Springer, Berlin/Heidelberg, 2001-
Kläntschi N., Lienemann P., Richner P., Vonmont H: Elementanalytik. Instrumenteller Nachweis und Bestimmung von Elementen und deren Verbindungen. Spektrum Analytik, 1996, Hardcover, 339 S., ISBN 3-86025-134-1.
Prerequisites / NoticeExcercises are integrated in the lectures. In addition, attendance in the lecture 529-0289-00 "Instrumental analysis of organic compounts" (4th semester) is recommended.
529-0058-AALAnalytical Chemistry II
Enrolment ONLY for MSc students with a decree declaring this course unit as an additional admission requirement.

Any other students (e.g. incoming exchange students, doctoral students) CANNOT enrol for this course unit.

This course does not offer a lecture of its own but it is linked to the course 529-0058-00L.
3 credits6RD. Günther, M.‑O. Ebert, P. Lienemann, G. Schwarz, R. Zenobi
AbstractEnhanced knowledge about the elemental analysis and spectrocopical techniques with close relation to practical applications. This course is based on the knowledge from analytical chemistry I. Separation methods are included.
Learning objectiveUse and applications of the elemental analysis and spectroscopical knowledge to solve relevant analytical problems.
ContentCombined application of spectroscopic methods for structure determination, and practical application of element analysis. More complex NMR methods: recording techniques, application of exchange phenomena, double resonance, spin-lattice relaxation, nuclear Overhauser effect, applications of experimental 2d and multipulse NMR spectroscopy, shift reagents. Application of chromatographic and electrophoretic separation methods: basics, working technique, quality assessment of a separation method, van-Deemter equation, gas chromatography, liquid chromatography (HPLC, ion chromatography, gel permeation, packing materials, gradient elution, retention index), electrophoresis, electroosmotic flow, zone electrophoresis, capillary electrophoresis, isoelectrical focussing, electrochromatography, 2d gel electrophoresis, SDS-PAGE, field flow fractionation, enhanced knowledge in atomic absorption spectroscopy, atomic emission spectroscopy, X-ray fluorescence spectroscopy, ICP-OES, ICP-MS.
Literaturegeneral: R. Kellner, J.-M. Mermet, M. Otto, H. M. Widmer (Eds.) Analytical Chemistry, Wiley-VCH, Weinheim, 1998;
XRF: R. Schramm, X-Ray Fluorescence Analysis: Practical and Easy, Fluxana, Kleve, 2012;
ICP-MS: R. Thomas, Practical Guide to ICP-MS - A Tutorial for beginners, 3rd Edition, CRC Press, Taylor & Francis Group, Boca Raton, 2013 (especially: chapters 1-15, 19 and 21).
Separation methods: S. Ahuja (Ed.), Chromatography and Separation Science, Volume 4 of series "Separation Science and Technology", Elsevier Academic Press, San Diego, 2003.
K. Robards, P. R. Haddad, and P. E. Jackson, Principle and Practise of Modern Chromatographic Methods, Academic Press, London, 1994.
F. Foret, L. Krivankova, and P. Bocek, Capillary Zone Electrophoresis, VCH, Weinheim (1993)
Prerequisites / NoticeNone.
529-0141-00LPhysical Methods for Inorganic Chemistry6 credits3GM. D. Wörle, D. Günther, J. Koch, R. Verel
AbstractIntroduction into the important methods for structural analysis (solid state NMR), crystal structure analysis and surface analysis techniques and their applications
Learning objectiveKnowledge in solid state NMR, crystal structure analysis and surface analytical techniques relevant for inorganic materials
ContentThis lecture course consists of three parts 1) Solid-state NMR 2) Surface and direct solid analysis 3) Crystal structure anaylsis. Most important fundamentals of the individual methods will be presented and details will be explained on most relevant inorganic applications
Lecture notesWill be given during the lectures
529-0169-00LInstrumental Analysis Restricted registration - show details 0 credits2SD. Günther
AbstractGroup seminar on elemental analysis and isotope ratio determinations using various plasma sources
Learning objectiveGroup seminar on elemental analysis and isotope ratio determinations using various plasma sources
ContentDevelopments in plasma mass spectrometry and alternative plasma sources
529-0199-00LInorganic and Organometallic Chemistry0 credits2KC. Copéret, H. Grützmacher, D. Günther, M. Kovalenko, A. Mezzetti, V. Mougel, A. Togni
AbstractWeekly one-hour lecture per year given by experts in the field to illustrate the latest development in inorganic/organometallic/solid-state chemistry (the fields of expertise include molecular and solid-state chemistry, main group and transition metal chemistry, analytical and computational chemistry as well as discussion on physical and catalytic properties of inorganic compounds); these lectures
Learning objectiveLearn the latest developments in inorganic/organometallic/solid-state chemistry from experts in the fields ; it also includes learning how to discuss chemistry with experts in an interactive fashion.