Name | Prof. Dr. Renato Zenobi |
Field | Analytische Chemie |
Address | Lab. für Organische Chemie ETH Zürich, HCI E 329 Vladimir-Prelog-Weg 1-5/10 8093 Zürich SWITZERLAND |
Telephone | +41 44 632 43 76 |
Fax | +41 44 632 12 92 |
renato.zenobi@org.chem.ethz.ch | |
Department | Chemistry and Applied Biosciences |
Relationship | Full Professor |
Number | Title | ECTS | Hours | Lecturers | |
---|---|---|---|---|---|
529-0041-00L | Modern Mass Spectrometry, Hyphenated Methods, and Chemometrics | 6 credits | 3G | R. Zenobi, M. Badertscher, B. Hattendorf, P. Sinués Martinez-Lozano | |
Abstract | Modern mass spectrometry, hyphenated analytical methods, speciation, methods of surface analysis, chemometrics. | ||||
Objective | Comprehensive knowledge about the analytical methods introduced in this course, and their applications. | ||||
Content | Coupling of separation with identification methods such as GC-MS, LC-MS, GC-IR, LC-IR, LC-NMR etc.; importance of speciation. Modern mass spectrometry: Time of flight and ion cyclotron resonance mass spectrometry, ICP-MS. Soft ionization methods, desorption methods, spray methods. Methods of surface analysis (ESCA, Auger, SIMS, raster microscopy methods). Employment of computer science for processing data in chemical analysis (chemometrics). | ||||
Lecture notes | lecture notes will be available in the lecture at production cost. | ||||
Literature | information about relevant literature will be available in the lecture & in the lecture notes. | ||||
Prerequisites / Notice | Exercises are an integral part of the lecture. Prerequisites: 529-0051-00 "Analytische Chemie I (3. Semester)" 529-0058-00 "Analytische Chemie II (4. Semester)" (or equivalent) | ||||
529-0043-00L | Analytical Strategy | 7 credits | 3G | R. Zenobi, M. Badertscher, P. S. Dittrich, D. Günther | |
Abstract | Problem-oriented development of analytical strategies and solutions. | ||||
Objective | Ability to create solutions for particular analytical problems. | ||||
Content | Individual development of strategies for the optimal application of chemical, biochemical, and physico-chemical methods in analytical chemistry solving predefined problems. Experts from industry and administration present particular problems in their field of activity. Principles of sampling. Design and application of microanalytical systems. | ||||
Lecture notes | Copies of problem sets and solutions will be distributed free fo charge | ||||
Prerequisites / Notice | Prerequisites: 529-0051-00 "Analytical Chemistry I (3. Semester)" 529-0058-00 "Analytical Chemistry II (4. Semester)" (or equivalent) | ||||
529-0051-AAL | Analytical Chemistry I Enrolment ONLY for MSc students with a decree declaring this course unit as an additional admission requirement. Any other students (e.g. incoming exchange students, doctoral students) CANNOT enrol for this course unit. | 3 credits | 6R | D. Günther, R. Zenobi | |
Abstract | Introduction into the most important spectroscopical methods and their applications to gain structural information. | ||||
Objective | Knowledge about the necessary theoretical background of spectroscopical methods and their practical applications | ||||
Content | Application oriented basics of organic and inorganic instrumental analysis and of the empirical employment of structure elucidation methods: Mass spectrometry: Ionization methods, mass separation, isotope signals, rules of fragmentation, rearrangements. NMR spectroscopy: Experimental basics, chemical shift, spin-spin coupling. IR spectroscopy: Revisiting topics like harmonic oscillator, normal vibrations, coupled oscillating systems (in accordance to the basics of the related lecture in physical chemistry); sample preparation, acquisition techniques, law of Lambert and Beer, interpretation of IR spectra; Raman spectroscopy. UV/VIS spectroscopy: Basics, interpretation of electron spectra. Circular dichroism (CD) und optical rotation dispersion (ORD). Atomic absorption, emission, and X-ray fluorescence spectroscopy: Basics, sample preparation. | ||||
Lecture notes | Script will be for the production price | ||||
Literature | - R. Kellner, J.-M. Mermet, M. Otto, H. M. Widmer (Eds.) Analytical Chemistry, Wiley-VCH, Weinheim, 1998; - D. A. Skoog und J. J. Leary, Instrumentelle Analytik, Springer, Heidelberg, 1996; - M. Hesse, H. Meier, B. Zeeh, Spektroskopische Methoden in der organischen Chemie, 5. überarbeitete Auflage, Thieme, Stuttgart, 1995 - E. Pretsch, P. Bühlmann, C. Affolter, M. Badertscher, Spektroskopische Daten zur Strukturaufklärung organischer verbindungen, 4. Auflage, Springer, Berlin/Heidelberg, 2001- Kläntschi N., Lienemann P., Richner P., Vonmont H: Elementanalytik. Instrumenteller Nachweis und Bestimmung von Elementen und deren Verbindungen. Spektrum Analytik, 1996, Hardcover, 339 S., ISBN 3-86025-134-1. | ||||
Prerequisites / Notice | Excercises are integrated in the lectures. In addition, attendance in the lecture 529-0289-00 "Instrumental analysis of organic compounts" (4th semester) is recommended. | ||||
529-0051-00L | Analytical Chemistry I | 3 credits | 3G | D. Günther, M.‑O. Ebert, R. Zenobi | |
Abstract | Introduction into the most important spectroscopical methods and their applications to gain structural information. | ||||
Objective | Knowledge about the necessary theoretical background of spectroscopical methods and their practical applications | ||||
Content | Application oriented basics of organic and inorganic instrumental analysis and of the empirical employment of structure elucidation methods: Mass spectrometry: Ionization methods, mass separation, isotope signals, rules of fragmentation, rearrangements. NMR spectroscopy: Experimental basics, chemical shift, spin-spin coupling. IR spectroscopy: Revisiting topics like harmonic oscillator, normal vibrations, coupled oscillating systems (in accordance to the basics of the related lecture in physical chemistry); sample preparation, acquisition techniques, law of Lambert and Beer, interpretation of IR spectra; Raman spectroscopy. UV/VIS spectroscopy: Basics, interpretation of electron spectra. Circular dichroism (CD) und optical rotation dispersion (ORD). Atomic absorption, emission, and X-ray fluorescence spectroscopy: Basics, sample preparation. | ||||
Lecture notes | Script will be for the production price | ||||
Literature | - R. Kellner, J.-M. Mermet, M. Otto, H. M. Widmer (Eds.) Analytical Chemistry, Wiley-VCH, Weinheim, 1998; - D. A. Skoog und J. J. Leary, Instrumentelle Analytik, Springer, Heidelberg, 1996; - M. Hesse, H. Meier, B. Zeeh, Spektroskopische Methoden in der organischen Chemie, 5. überarbeitete Auflage, Thieme, Stuttgart, 1995 - E. Pretsch, P. Bühlmann, C. Affolter, M. Badertscher, Spektroskopische Daten zur Strukturaufklärung organischer verbindungen, 4. Auflage, Springer, Berlin/Heidelberg, 2001- Kläntschi N., Lienemann P., Richner P., Vonmont H: Elementanalytik. Instrumenteller Nachweis und Bestimmung von Elementen und deren Verbindungen. Spektrum Analytik, 1996, Hardcover, 339 S., ISBN 3-86025-134-1. | ||||
Prerequisites / Notice | Excercises are integrated in the lectures. In addition, attendance in the lecture 529-0289-00 "Instrumental analysis of organic compounts" (4th semester) is recommended. | ||||
529-0280-00L | Analytical Chemistry Seminar | 0 credits | 1K | R. Zenobi, P. S. Dittrich | |
Abstract | Analytical Chemistry Seminar | ||||
Objective | Presentation and discussion of current research topics in analytical chemistry | ||||
Content | Presentation and discussion of current research topics in analytical chemistry | ||||
529-0290-00L | Organic Chemistry (Seminar) | 0 credits | 2S | E. M. Carreira, J. W. Bode, F. Diederich, P. S. Dittrich, D. Hilvert, H. Wennemers, R. Zenobi | |
Abstract | |||||
Objective | |||||
529-0299-00L | Organic Chemistry | 0 credits | 1.5K | J. W. Bode, E. M. Carreira, P. Chen, F. Diederich, P. S. Dittrich, D. Hilvert, H. Wennemers, R. Zenobi | |
Abstract | |||||
Objective |